MW ON
Probe: 3.2 mm DNP HCN mode, AVNeo console
Sample: sample 12 HPMC-AS with 20 mM AMUPol in D2O:H2O 9:1 (solid:solution 1:4)
Saphire rotor
MAS = 8 kHz, BP = 2173 mB, DP = 967 mB
Tsample = 96 K, flow = 1600 l/h, Tbearing = 96 K, Tdrive = 97.5 K
I = 100 mA
Tcavity = 22.5 C
epsilon 25

1H pulses and SPINAL dec 100 kHz at 67 W, o2 1H offset = -64442 Hz, pcpd2 = 4.8 us
1H CP 100 kHz matched to 13C at 60 W (71 kHz), ramp 70.100.100 on 1H
3 s d1 (larger than 5 x T1, data in 128)
1 ms CP

best SNR
MWoff in 180